Section 60.133 - Test methods and procedures(a) In conducting performance tests required in § 60.8 , the owner or operator shall use as reference methods and procedures the test methods in appendix A of this part or other methods and procedures as specified in this section, except as provided in § 60.8(b) .(b) The owner or operator shall determine compliance with the particulate matter standards in § 60.132 as follows: (1) Method 5 shall be used to determine the particulate matter concentration during representative periods of charging and refining, but not during pouring of part of the production cycle. The sampling time and sample volume for each run shall be at least 120 minutes and 1.80 dscm (63.6 dscf).(2) Method 9 and the procedures in § 60.11 shall be used to determine opacity.54 FR 6667, Feb. 14, 1989, as amended at 65 FR 61756 , Oct. 17, 2000