Ariz. Admin. Code § tit. 9, ch. 14, art. 6, tbl. 6.2.B
1. Microbiology of Wastewater and Sewage Sludge | |||
Description | Reference | Method/s | Fee Per Method |
Ascaris lumbricoides | C8 | 10550 | $228 |
P3 | UofA2000 | $228 | |
Coliforms, Fecal, number per 100 ml or number per gram dry weight, by Membrane Filter | C | 9222D (2006) | $228 |
Coliforms, Fecal, by Multiple Tube Fermentation (may be used for sewage sludge), number per 100 ml by MPN | C | 9221C, E (2006) | $228 |
Coliforms, Total, by Membrane Filter | C | 9222B (2006) | $228 |
Coliforms, Total, by Multiple Tube Fermentation | C | 9221B (2006) | $228 |
Control of pathogens and vectors in sewage | E3 | 625/R-92/013 | $76 |
Cryptosporidium | A4.32 | 1622 | $381 |
Cryptosporidium and Giardia E. coli, number per 100 ml, MPN multiple tube | A4.39 | 1623 | $381 |
C | 9711B (2011) | $381 | |
P2 | 600/R-95/178 | $381 | |
C | 9222B (2006) | $228 | |
E. coli, number per 100 ml, MPN multiple tube/multiple well | C | 9223B (2004) | $228 |
E. coli by m-ColiBlue | C1 and Z6 | Hach 10029 | $228 |
Enterococci, number per 100 ml MF | C | 9230C (2007) | $228 |
Escherichia coli by Colilert MPN, in conjunction with SM 9221B and 9221C | C | 9223B (2004) | $152 |
Escherichia coli in conjunction with SM 9221B and 9221C | C | 9221F (2006) | $152 |
Entamoeba histolytica | C | 9711C (2011) | $228 |
Enteric viruses | I | D4994-89 | $381 |
Enteric viruses in sewage sludge | E3 | EPA 625/R-92/103 | $381 |
Fecal Coliforms by Colilert-18 (APP and Reuse only) | C | 9020B (2005)/9223B (2004) | $152 |
Fecal Coliforms by Colilert-18 (NPDES-ATP Permits only) | C | 9020B (2005)/9223B (2004) | $152 |
Fecal Coliforms in sewage sludge by MTF | Z1 | EPA 1681 | $228 |
Helminth Ova in sludge | Z4 | 600/1-87-014 | $381 |
Salmonella in sludge MPN | E5 | 9260D (1988) | $228 |
Salmonella in Sewage Sludge (Biosolids) by Modified MSRV | A4.34 | 1682 | $228 |
Streptococcus, Fecal, by Membrane Filter | C | 9230C (2007) | $194 |
Streptococcus, Fecal, by Multiple Tube Fermentation | C | 9230B (2007) | $194 |
Viruses | C | 9510 (2011) | $381 |
P | Methods for Virology | $381 | |
P2 | 600/R-95/178 | $381 | |
2. Wastewater Inorganic Chemistry, Nutrients and Demand | |||
Acid Mine Drainage | A4.27 | 1627 | $303 |
Acidity | C | 2310B (2011) | $39 |
Alkalinity, Total | A | 310.2 (1974) | $19 |
C | 2320B (2011) | $19 | |
Ammonia | A2 | 350.1 (2.0) | $39 |
C | 4500-NH3 B (2011) | $39 | |
4500-NH3 C (2011) | $39 | ||
4500-NH3 D (2011) | $39 | ||
4500-NH3 E (2011) | $39 | ||
4500-NH3 G (2011) | $39 | ||
C1 | Hach 10205 | $39 | |
Ammonia in sludge only | E5 | 4500-NH3B&C (1990) | $39 |
Biochemical Oxygen Demand/Carbonaceous Biochemical Oxygen Demand | C | 5210B (2011) | $152 |
C3 | Hach 10360 | $152 | |
Boron | A1 A4.10 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.5 (4.2) | $10 | ||
C | 4500-B B (2011) | $76 | |
Bromide Calcium | A2 | 300.0 (2.1) | $26 |
A5 | 300.1 (1.0) | $26 | |
A1 A4.10 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
200.5 (4.2) | $10 | ||
C | 3111B (2011) | $26 | |
3500-Ca B (2011) | $39 | ||
Carbon, Total Organic (TOC) | C | 5310 B (2011) | $39 |
5310 C (2011) | $39 | ||
5310D (2011) | $39 | ||
Chemical Oxygen Demand | A | 410.3 (1978) | $39 |
A2 | 410.4 (2.0) | $76 | |
C C1 | 5220 B (2011) | $39 | |
5220 C (2011) | $39 | ||
5220 D (2011) | $76 | ||
Hach 8000 | $39 | ||
Chloride | A2 | 300.0 (2.1) | $26 |
A5 | 300.1 (1.0) | $26 | |
C | 4500-Cl B (2011) | $39 | |
4500-Cl C (2011) | $39 | ||
4500-Cl D (2011) | $39 | ||
4500-Cl E (2011) | $39 | ||
Chlorine, Total Residual Color Cyanide, Available Cyanide, Free | C | 4500-Cl B (2011) | $39 |
4500-Cl C (2011) | $39 | ||
4500-Cl D (2011) | $39 | ||
4500-Cl E (2011) | $39 | ||
4500-Cl F (2011) | $39 | ||
4500-Cl G (2011) | $39 | ||
C1 | Hach 10014 | $39 | |
C | 2120 B (2011) | $32 | |
C | 4500-CN G (2011) | $76 | |
E7 | Kelada-01 | $76 | |
Y | OIA-1677-09 (8/99) | $76 | |
Y | OIA-1677-09 (8/99) | $76 | |
Cyanide, Total Fluoride | A2 | 335.4 (1.0) | $76 |
A6 | QuickChem 10-204-00-1-X (2.1) | $76 | |
C | Combination of 4500-CN B (2011) and 4500-CN C (2011), followed by 4500-CN D (2011), 4500-CN E (2011), or 4500-CN F (2011) | $89 | |
E7 | Kelada-01 | $76 | |
A2 | 300.0 (2.1) | $26 | |
A5 | 300.1 (1.0) | $26 | |
C | 4500-F B (2011) | $39 | |
4500-F C (2011) | $39 | ||
4500-F D (2011) | $39 | ||
4500-F E (2011) | $39 | ||
Hardness | A | 130.1 (1976) | $10 |
A1 A4.10 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
200.5 (4.2) | $10 | ||
C | 2340B (2011) | $39 | |
2340C (2011) | $39 | ||
Kjeldahl, Total Nitrogen | A | 351.1 (1978) | $76 |
A2 | 351.2 (2.0) | $76 | |
C Z9 | Combination of 4500-NH3 B (2011) and either 4500-Norg B (2011) or 4500-Norg C (2011) | $115 | |
4500-NH3 C (2011) | $39 | ||
4500-NH3 D (2011) | $39 | ||
4500-NH3 E (2011) | $39 | ||
4500-NH3 F (2011) | $39 | ||
4500-NH3 G (2011) | $39 | ||
4500-NH3 H (2011) | $39 | ||
PAI-DK01 (12/94) | $76 | ||
Z10 | PAI-DK02 (12/94) | $76 | |
Z11 | PAI-DK03 (12/94) | $76 | |
Methylene Blue Active Substances | C | 5540C (2011) | $39 |
Nitrate (as N) Nitrate-Nitrite (as N) Nitrite (as N) | A | 352.1 (1971) | $76 |
A2 | 300.0 (2.1) | $26 | |
A5 | 300.1 (1.0) | $26 | |
C | 3500-NO3 D (2011) | $39 | |
A2 | 300.0 (2.1) | $26 | |
353.2 (2.0) | $76 | ||
A5 | 300.1 (1.0) | $26 | |
C | 4500-NO3 E (2011) | $76 | |
4500-NO3 F (2011) | $76 | ||
4500-NO3 H (2011) | $76 | ||
A2 A5 | 300.0 (2.1) | $26 | |
353.2 (2.0) | $76 | ||
300.1 (1.0) | $26 | ||
C | 4500-NO2 B (2011) | $76 | |
4500-NO3 E (2011) | $76 | ||
4500-NO3 F (2011) | $76 | ||
Oil and Grease and Total Petroleum Hydrocarbons | A4.24 | 1664 Rev B | $76 |
C | 5520B (2011) | $76 | |
Orthophosphate | A | 365.3 (2.0) | $76 |
A2 | 300.0 (2.1) | $26 | |
365.1 (2.0) | $76 | ||
A5 | 300.1 (1.0) | $26 | |
C | 4500-P E (2011) | $76 | |
4500-P F (2011) | $76 | ||
Oxygen-consumption Rate (SOUR) | C | 2710B (2011) | $39 |
Oxygen, Dissolved pH (Hydrogen Ion) | C C1 | 4500-O B (2011) | $26 |
4500-O C (2011) | $26 | ||
4500-O D (2011) | $26 | ||
4500-O E (2011) | $26 | ||
4500-O F (2011) | $26 | ||
4500-O G (2011) | $26 | ||
1002-8-2009 | $26 | ||
C3 | Hach 10360 | $26 | |
A | 150.2 | $39 | |
C | 4500-H B (2011) | $39 | |
Phenols | A | 420.1 (1978) | $116 |
A2 | 420.4 (1.0) | $116 | |
C A | 5530 B (2010) | $116 | |
5530 D (2010) | $116 | ||
Phosphorus, Total | 365.3 (1978) | $76 | |
365.4 (1974) | $76 | ||
A1 | 200.7 (4.4) | $10 | |
A2 | 365.1 (2.0) | $76 | |
C A1 C | 4500-P B (2011) | $76 | |
4500-P E (2011) | $76 | ||
4500-P F (2011) | $76 | ||
4500-P G (2011) | $76 | ||
4500-P H (2011) | $76 | ||
Potassium Residue, Filterable (TDS) Residue, Nonfilterable (TSS) | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
3111B (2011) | $26 | ||
3500-K B (2011) | $26 | ||
C | 2540C (2011) | $39 | |
E8 | I-1750-85 | $39 | |
C | 2540D (2011) | $39 | |
Residue, Settleable Solids | C | 2540F (2011) | $39 |
Residue, Total | C | 2540B (2011) | $39 |
Residue, Volatile Silica, Dissolved Sodium | A | 160.4 (1971) | $39 |
C | 2540E (2011) | $39 | |
A1 A4.10 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
200.5 (4.2) | $10 | ||
C | 4500-SiO2 B (2011) | $76 | |
4500-SiO2 C (2011) | $76 | ||
4500-SiO2 E (2011) | $76 | ||
4500-SiO2 F (2011) | $76 | ||
A1 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C C | 3500-Na B (2011) | $26 | |
3500-Na D (2011) | $26 | ||
3111B (2011) | $26 | ||
Sodium Azide | 4110C (2011) | $76 | |
Specific Conductance | A | 120.1 (1982) | $39 |
C | 2510B (2011) | $39 | |
Sulfate Sulfide (includes total and soluble) Sulfite | A2 | 300.0 (2.1) | $26 |
375.2 (2.0) | $76 | ||
A5 | 300.1 (1.0) | $26 | |
C | 4500-SO4 C (2011) | $76 | |
4500-SO4 D (2011) | $76 | ||
4500-SO4 E (2011) | $76 | ||
4500-SO4 F (2011) | $76 | ||
4500-SO4 G (2011) | $76 | ||
4500-S2- B (2011) | $39 | ||
C | 4500-S2- D (2011) | $76 | |
4500-S2- F (2011) | $39 | ||
4500-S2- G (2011) | $39 | ||
C1 | Hach 8131 | $39 | |
C | 4500-SO3 B (2011) | $76 | |
Temperature, Degrees Celsius | C | 2550B (2010) | $13 |
Total, Fixed and Volatile Solids in Solid and Semisolid Samples in Sludge | C | 2540G (2011) | $39 |
Turbidity, NTU | A2 | 180.1 (2.0) | $39 |
C | 2130B (2011) | $39 | |
3. Metals in Wastewater | |||
a. Sample Preparation for Metals in Wastewater | |||
Acid Extractable Metals | C | 3030C (2004) | $7 |
Digestion for Metals | C | 3030D (2004) | $7 |
Microwave Digestion | E6 | CEM Microwave Digestion | $7 |
Nitric Acid | C | 3030E (2004) | $7 |
Nitric Acid/Hydrochloric Acid | C | 3030F (2004) | $7 |
Nitric Acid/Perchloric Acid | C | 3030H (2004) | $7 |
Nitric Acid/Perchloric Acid/Hydrofluoric Acid | C | 3030I (2004) | $7 |
Nitric Acid/Sulfuric Acid | C | 3030G (2004) | $7 |
Preliminary Filtration | C | 3030B (2004) | $7 |
b. Methods to Analyze Metals in Wastewater | |||
Aluminum | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3113B (2010) | $26 | |
3111D (2011) | $26 | ||
Antimony | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
A4.25 | 1638 | $26 | |
C | 3111B (2011) | $26 | |
3113B (2010) | $26 | ||
Arsenic | A | 206.5 (1978) | $39 |
A1 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3113B (2010) | $26 | |
3500-As B (2011) | $76 | ||
Barium | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111D (2011) | $26 | |
3113B (2010) | $26 | ||
Beryllium | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111D (2011) | $26 | |
3111E (2011) | $26 | ||
3113B (2010) | $26 | ||
Cadmium | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
A4.25 | 1638 | $26 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
3500-Cd D (2011) | $76 | ||
Chromium (VI) Hexavalent Chromium, Total | A1 | 218.6 (3.3) | $26 |
C | 3500-Cr B (2011) | $39 | |
3111C (2011) | $26 | ||
A1 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
3500-Cr B (2011) | $76 | ||
Cobalt | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
Copper | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
A4.25 | 1638 | $26 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
3500-Cu B (2011) | $76 | ||
3500-Cu C (2011) | $76 | ||
Gold | A | 231.2 (1978) | $26 |
A1 | 200.8 (5.4) | $26 | |
C | 3111B (2011) | $26 | |
Iridium | A | 235.2 (1978) | $26 |
C | 3111B (2011) | $26 | |
Iron | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
3500-Fe B (2011) | $76 | ||
Lead | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
A4.25 | 1638 | $26 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
3500-Pb B (2011) | $76 | ||
Lithium | A1 | 200.7 (4.4) | $10 |
Magnesium | A1 A4.10 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.5 (4.2) | $10 | ||
C | 3111B (2011) | $26 | |
Manganese | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111B (2011) | $26 | |
3113B (2010) | $26 | ||
3500-Mn B (2011) | $76 | ||
Mercury | A | 245.2 (1974) | $52 |
A1 A4.17 | 200.7 (4.4) | $10 | |
245.1 (3.0) | $52 | ||
1631E | $152 | ||
A4.23 | 245.7 (2.0) | $15 | |
C | 3112B (2011) | $52 | |
Molybdenum | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111D (2011) | $26 | |
3113B (2010) | $26 | ||
Nickel | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
A4.25 | 1638 | $26 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
Osmium | A | 252.2 (1978) | $26 |
C | 3111D (2011) | $26 | |
Palladium | A | 253.2 (1978) | $26 |
C | 3111B (2011) | $26 | |
Platinum | A | 255.2 (1978) | $26 |
C | 3111B (2011) | $26 | |
Rhodium | A | 265.2 (1978) | $26 |
C | 3111B (2011) | $26 | |
Ruthenium | A | 267.2 (1978) | $26 |
C | 3111B (2011) | $26 | |
Selenium | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3113B (2010) | $26 | |
3114B (2011) | $76 | ||
Silver | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3113B (2010) | $26 | ||
Strontium | A1 | 200.7 (4.4) | $10 |
C | 3111B (2011) | $26 | |
3500-Sr B (2011) | $26 | ||
3500-Sr C (2011) | $20 | ||
3500-Sr D (2011) | $26 | ||
Thallium | A | 279.2 (1978) | $26 |
A1 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
A4.25 | 1638 | $26 | |
C | 3111B (2011) | $26 | |
Tin | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
200.9 (2.2) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111B (2011) | $26 | |
3113B (2010) | $26 | ||
Titanium | A | 283.2 (1978) | $26 |
A1 C | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
3111D (2011) | $26 | ||
Vanadium | A1 | 200.7 (4.4) | $10 |
200.8 (5.4) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
C | 3111D (2011) | $26 | |
3500-V B (2011) | $76 | ||
Zinc | A | 289.2 (1978) | $26 |
A1 | 200.7 (4.4) | $10 | |
200.8 (5.4) | $26 | ||
A4.10 | 200.5 (4.2) | $10 | |
A4.25 | 1638 | $26 | |
C | 3111B (2011) | $26 | |
3111C (2011) | $26 | ||
3500 Zn B (2011) | $76 | ||
4. Aquatic Toxicity Bioassay of Wastewater | |||
Toxicity, Acute | M1 | EPA/600/4-90/027F | $194 |
Z12 | 821-R-02-012 | $194 | |
Toxicity, Chronic | N1 | EPA/600/4-91/002 | $194 |
Z2 Z13 | 821-R-02-013 | $194 | |
Lozarchak, J. 2001 | $194 | ||
5. Organic Chemicals of Wastewater | |||
Volatile Organics for Pharmaceuticals | D3 | 524.2 (4.1) | $152 |
Purgeable Hydrocarbons | E | 601 | $76 |
Purgeable Aromatics | E | 602 | $76 |
Acrolein and Acrylonitrile | E | 603 | $76 |
624 | $152 | ||
Phenols | E | 604 | $116 |
Benzidines | E | 605 | $116 |
Phthalate ester | E | 606 | $116 |
Nitrosamines | E | 607 | $116 |
Organochlorine Pesticides and PCBs Nitroaromatics and Isophorone | E | 608 | $152 |
E2 | 608.1 | $152 | |
608.2 | $152 | ||
E4 | 608 (3M) | $152 | |
E | 609 | $116 | |
PAHs | E | 610 | $116 |
Haloethers | E | 611 | $116 |
Chlorinated Hydrocarbons | E | 612 | $116 |
2, 3, 7, 8-Tetrachlorodibenzo-p-Dioxin | E | 613 | $457 |
Chlorinated Herbicides | E2 | 615 | $116 |
Organohalide Pesticides and PCB | E2 | 617 | $116 |
Triazine Pesticides | E2 | 619 | $116 |
Thiophosphate Pesticides | E2 | 622.1 | $116 |
Purgeables | E | 624 | $152 |
Base/Neutrals and Acids (all analytes excluding pesticides) | E | 625 | $152 |
Base/Neutrals and Acids (pesticides only) | E | 625 | $152 |
Carbamate and Urea Compounds | E2 | 632 | $116 |
Tetra- through Octa-Chlorinated Dioxins and Furans | A4.22 | 1613 Rev B (10/94) | $258 |
VOCs by Isotope Dilution GC/MS | E | 1624B | $152 |
Semivolatile Organic Compounds by Isotope Dilution GC/MS | E | 1625B | $152 |
Organophosphorus Pesticides VOCs Specific to the Pharmaceutical Manufacturing Industry by Isotope Dilution GC/MS | E1 | 1657 | $116 |
E2 | 614 | $116 | |
614.1 | $116 | ||
622 | $116 | ||
K1 | 1666 (A) | $152 | |
Herbicides | C | 6640B (2006) | $116 |
Ethylene Glycol | K | BLS-188 | $152 |
6. Radiochemistry of Wastewater | |||
Alpha-Total pCi per liter | C | 7110B (2011) | $206 |
L | 900.0 | $206 | |
Alpha Counting Error, pCi per liter | C | 7110B (2011) | $206 |
Beta-Total pCi per liter | C | 7110B (2011) | $206 |
L | 900.0 | $206 | |
Beta Counting Error, pCi | C | 7110B (2011) | $206 |
Radium, Total pCi per liter | C | 7500-Ra B (2011) | $206 |
L | 903.0 | $206 | |
Radium | C | 7500-Ra C (2011) | $206 |
L | 903.1 | $206 | |
Ariz. Admin. Code tit. 9, ch. 14, art. 6, tbl. 6.2.B